引用本文:秦兴秀,王来梁,杨敏娜.重点行业企业用地地下水中挥发性有机物分析方法探究[J].环境监控与预警,2021,13(1):25-29
QIN Xing-xiu,WANG Lai-liang,YANG Min-na.Study on Analytical Methods of Volatile Organic Compounds in Groundwater of Enterprise Land Pollution Investigation[J].Environmental Monitoring and Forewarning,2021,13(1):25-29
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重点行业企业用地地下水中挥发性有机物分析方法探究
秦兴秀,王来梁,杨敏娜
作者单位
秦兴秀,王来梁,杨敏娜 江苏省地质调查研究院江苏 南京 210018 
摘要:
通过优化顶空条件(氯化钠加入量、顶空平衡温度、顶空平衡时间),对采用顶空-气相色谱-质谱联用法测定地下水中55种挥发性有机物的方法进行探究。结果表明:该方法检出限为0.24~2.30μg/L,相对标准偏差为0.76%~13.2%,实际样品加标回收率为82.7%~119%。该方法具有较高的灵敏度、精密度和准确度,操作简便,可用于企业用地地下水中挥发性有机物的检测。
关键词:  顶空-气相色谱-质谱联用法  地下水  挥发性有机物  企业用地
DOI:
分类号:X832;O657.6
文献标识码:B
基金项目:耕地环境污染调查成果在基本农田保护修复中的应用试点研究基金资助项目(苏财建〔2017〕123号)
Study on Analytical Methods of Volatile Organic Compounds in Groundwater of Enterprise Land Pollution Investigation
QIN Xing-xiu,WANG Lai-liang,YANG Min-na
Abstract:
In this paper, the headspace gas chromatography mass spectrometry method was established to determine 55 volatile organic compounds in groundwater by optimizing conditions of headspace(content of sodium chloride, equilibrium temperature, equilibrium time). The results showed that the detection limits were in the range of 0.24 ~ 2.30 μg/L, the relative standard deviation was 0.76% ~ 13.2% and the average recoveries ranged from 82.7% to 119%. This method was simple with high sensitivity, precision and accuracy and was suitable for simultaneous determination of various volatile organic compounds in groundwater of enterprise land.
Key words:  Headspace gas chromatography mass spectrometry  Groundwater  Volatile organic compounds  Enterprise land